Method of blood dichlorobromomethane measurement
Year:
2011
Autors:
Professor Nina V. Zaitseva, PhD, DSc, Professor Tatyana S. Ulanova, PhD, DSc, Nurislamova T.V., Popova N. A.
FIELD: medicine.
SUBSTANCE: method starts with blood sample alkalisation with 10% sodium hydroxide to pH 8-10; dichlorobromomethane is recovered from the sample by hexane extraction; the extract is separated centrifugally at 7000-7500 rpm and analysed with gas chromatography in a partition gas chromatograph with an electron capture detector, while dichlorobromomethane is measured by a calibration diagram.
EFFECT: high sensitivity and accuracy of the method for blood dichlorobromomethane measurement.
Registered RU 2 416 798 C1
Application: 2009148379/15, 24.12.2009
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 2417086.pdf | 522.61 KB |
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